Column: dB-XlB
15 m x 0.18 mm, 0.07 um

Agilent Technologies custom column

Carrier: Hydrogen at 72 cm/s at 100 °C (4.0 mL/min),

            constant flow mode

Oven: 100 °C for 0.5 min

          100 °C to 300 °C at 30 °C/min

          300 °C for 5 min

Injection: Split, 250 °C

              Split ratio 20:1

Detector: ECD, 300 °C

              Peak, Congener (2.5 mg/mL)

Sample: 1 µL

Special thanks to AccuStandard, Inc. of New Haven, CT,
for PBDE standards.